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RAS Chemistry & Material ScienceЖурнал общей химии Russian Journal of General Chemistry

  • ISSN (Print) 0044-460X
  • ISSN (Online) 3034-5596

Synthesis and Study of Iron-Graphene Composites

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PII
S3034559625090137-1
DOI
10.7868/S3034559625090137
Publication type
Article
Status
Published
Authors
A. A. Arbuzov
  • Affiliation: Federal Research Center of Problems of Chemical Physics and Medicinal Chemistry, Russian Academy of Sciences
I. D. Shamov
  • Affiliation: Federal Research Center of Problems of Chemical Physics and Medicinal Chemistry, Russian Academy of Sciences
M. A. Blagov
  • Affiliation: Federal Research Center of Problems of Chemical Physics and Medicinal Chemistry, Russian Academy of Sciences
M. V. Lotockij
  • Affiliation:
    Federal Research Center of Problems of Chemical Physics and Medicinal Chemistry, Russian Academy of Sciences
    HySA Systems Centre of Competence, University of the Western Cape
B. P. Tarasov
  • Affiliation: Federal Research Center of Problems of Chemical Physics and Medicinal Chemistry, Russian Academy of Sciences
Volume/ Edition
Volume 95 / Issue number 9-10
Pages
472-480
Abstract
Iron-graphene composites were synthesized by heat treatment of a mixture of iron (III) nitrate and graphite oxide in an argon flow, followed by reduction in a hydrogen flow. The composites were characterized by elemental analysis, thermogravimetry, scanning electron microscopy with energy-dispersive X-ray spectra and construction of maps of the spatial distribution of components, X-ray phase analysis, and Mossbauer spectroscopy. It was shown that the synthesized composites are sheets of a graphene-like material with iron-containing nanoparticles deposited on them, the size of which depends on the concentration of the iron compound in the original mixture. Iron nanoparticles in the obtained composites are rapidly oxidized upon short-term contact with air and can be restored by cyclic treatment at 400°C, including vacuuming the composite followed by exposure to hydrogen under pressure.
Keywords
железо наночастицы оксид графита графеноподобный материал восстановление композит
Date of publication
21.12.2025
Year of publication
2025
Number of purchasers
0
Views
44

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