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RAS Chemistry & Material ScienceЖурнал общей химии Russian Journal of General Chemistry

  • ISSN (Print) 0044-460X
  • ISSN (Online) 3034-5596

Synthesis and physicochemical properties of tin(IV), zirconium(IV), and hafnium(IV) 2(3),9(10),16(17),23(24)-tetrakis-(4-tritylphenoxy)phthhalocyaninates

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PII
10.31857/S0044460X2307017X-1
DOI
10.31857/S0044460X2307017X
Publication type
Article
Status
Published
Authors
M. V. Kozlova
  • Affiliation: Ivanovo State University of Chemistry and Technology
N. E Galanin
  • Affiliation: Ivanovo State University of Chemistry and Technology
Volume/ Edition
Volume 93 / Issue number 7
Pages
1124-1131
Abstract
The reaction of 4-tritylphenoxyphthalonitrile with SnCl2, ZrCl4 and HfCl4 in the presence of urea under ammonium molybdate catalysis was used to synthesize tetrakis-(4-tritylphenoxy)phthalocyaninates of tin(IV), zirconium(IV), and hafnium(IV). The complexes were characterized by spectral methods of analysis, including mass spectrometry, 1Н NMR, vibrational and electron spectroscopy. All of them form J -type dimer associates in chloroform at concentrations up to ~1.5×10-6 mol/L and lower, are not associated in a mixture of toluene and pyridine up to concentrations of ~3×10-5 mol/L and higher, have catalytic activity in electroreduction reactions of molecular oxygen. The complexes of zirconium and hafnium showed the highest activity. Tin and zirconium complexes are thermally stable in an inert atmosphere up to a temperature of 200°C.
Keywords
4-тритилфеноксифталонитрил тетракис-(4-тритилфенокси)фталоцианинаты олово цирконий гафний электрокатализ термическая устойчивость
Date of publication
17.09.2025
Year of publication
2025
Number of purchasers
0
Views
15

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